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NETZSCH sta 449f3 synchronous thermal analyser
Sta 449f3 Synchronous Thermal Analyser, supplied by NETZSCH, used in various techniques. Bioz Stars score: 90/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
https://www.bioz.com/product/sta+449f3+synchronous+thermal+analyser/dsc+204/10__1016_slash_j__ceramint__2024__12__319-113-4-9
Average 90 stars, based on 1 article reviews
sta 449f3 synchronous thermal analyser - by Bioz Stars, 2026-09
90/100 stars

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Article Title: Synthesizing mixed-phase TiO2 semiconductor catalysts via microwave-assisted rutile seed crystal: A new approach
Article Snippet: The study introduces a microwave-assisted rutile seed crystal (RS) method to synthesise mixed-phase TiO2 nanoparticles, controlling the rutile TiO2 (TiO2-R) phase content (γR) from 33.0 % to 99.3 % by adjusting the doping level of RS to 20.0 wt% in the metatitanic acid (MA).. The sample, designated as MA-20, with the highest oxygen vacancy (Ov) concentration of 38.56 %, demonstrated over 99 % microwave absorption (minimum reflection loss (RL) − 56.8 dB) and a heating rate of 0.836 C/s under 2000 W and 20 g. RS enhanced the dielectric property of MA, facilitating phase transition from anatase TiO2 (TiO2-A) to TiO2-R above 600 C, with critical temperatures between 800 and 1000 C. MA-20, with a surface area of 1.9226 m2/g and pore size distribution of 9.0851 nm, showed that higher RS doping levels promoted phase transition and grain growth, thereby enhancing the crystallinity and charge transfer efficiency.. More than 50 % of MA-20 particles were under 10 nm, and 94 % were below 100 nm, confirming the synthesis of TiO2 nanomaterials.



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